SINGLE DISC ELECTRODESTM (SDEs)
(Microfrabricated Single Disc Electrodes)

MDEA DEVICES

Number of Discs

Disc dimensions

Active Area

Conductor

SDE Au 0.1

1 disc

0.357 cm diameter

0.10 cm2

Au

SDE Au 0.01

1 disc

0.036 cm diameter

0.01 cm2

Au

SDE Pt 0.1

1 disc

0.357 cm diameter

0.10 cm2

Pt

SDE Pt 0.01

1 disc

0.036 cm diameter

0.01 cm2

Pt


 




SDE Brochure (PDF)

SDE Prices

Price List

Introduction and Background

Applications of SDEs

Technical Specifications

SDE Accessories

Methods

Application Notes

Introduction and Background

Ø Single Disc Electrodes (SDEs) are inert, microfabricaed electrodes formed from a microlithographically patterned insulator-on-conductor-on-insulator configuration. They are designed for the study of electrical and electrochemical properties of thin polymeric films and coatings, for applications in microelectrochemistry, for electrical/electrochemical impedance spectroscopy, and for chemical and biological sensor development.
Ø Microfabricated from 100 nm magnetron sputter-deposited gold (Au), e-gun vapor-deposited platinum (Pt), or conductive indium tin oxide (ITO) on an electronics grade borosilicate glass, these devices are supplied in two disc diameters. A 500nm thin silicon nitride layer is applied over the conductor and is microlithographically windowed using reactive ion etching to reveal a precisely patterned window to the metal beneath and a bonding pad. SDEs are avalable as un-packaged die.
Ø SDE chips of gold, platinum or ITO are available with 0.357 cm diameter (A=0.10 cm2) or 0.0357 cm diameter (A=0.01cm2 ) discs.
Ø In research and product development, these devices are widely used for electrochemical, bio-electrochemical, biofuel cell, electrical and electrochemical impedacne spectroscopy.

Ø These electrodes/devices are particulary necessary when a precisely defined area electrode is required.

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Applications of SDEs

Applications of MDEAs in research and product development include:

Ø As a substrate electrode for the deposition of electroactive polymer thin films, alkane thiol monlayers, for electrodeposition of carbon nanotubes, for SAM innobilization of enzymes and enzyme-linked antibodies for biosensor development.

Ø For the study of electrical and electrochemical impedance spectroscopy of organic thin films and coatings and carbon nanotubes.

Ø As a capacitance probe during the deposition or cure of an organic thin film or polymer e.g. Films based on Langmuir-Blodgett thin film deposition or cure of an epoxy.
Ø In modern microelectrochemistry -- as generator and collector electrodes in electrochemical amplification or in the performance of electroanalysis in high impedance environments. The microdisc electrode format allows accommodates radial diffusion .
Ø In conductimetry studies. To determine the conductance of low conductivity media and in conductimetric titrations.
Ø In coatings research and development. For example, to study the transport of water into and through a coating or to study the physical aging of the polymer upon environmental exposure or accelerated aging.
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Technical Specifications

Ø Chip Substrate:

Schott D263 Borosilicate Glass



Dielectric Constant, Epsilon(r) at 1 MHz

6.7


Dielectric Loss Angle, tan delta, at 1 MHz

61 x 10-4


Electrical Resistivity (50 Hz) (250 C)

1.6 x 10^8 ohm cm


Coefficient of Linear Thermal Expansion, * 20-300 Deg C

7.2 x 10^-6 K^-1


Refractive Index at 20 C, ne ( Lambda = 546.1 nm)

1.5249




Ø Metallization:

100 Å Ti|W / 1000 Å Au or Pt and ITO = 10 Ohms/sq





Ø Insulating Top Layer:

Silicon Nitride (Si3N4)







No of Discs

Electroactive Area (cm2)

Geometric Area (cm2)

Ø SDE 0.10

A single disc, 0.357 cm diameter.

1

1.0 x10-1

1.0 x10-1

Ø SDE 0.01

A single disc, 0.0357 cm diameter

1

1.0 x10-2

1.0 x10-2






Ø SDE Chip Dimensions

Un-packaged Die

Packaged Die


(l x w x t)

(l x w x t)

SDE X.XX

1.00 x 0.50 x 0.05 cm

N.A.




Ø Packaging



Electrode Body:

N.A.

Encapsulant:

N.A.

Leadwires:

N.A.

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MDEA Accessories


Wand

Test Clip

Lead Length

4.5 cm

N/A

Connector Type

Gold Plated Pins

Gold Plated Pins

Number of Conductors

4

4

Lead

Rigid Wand - PCB

Spring Loaded Pinch Clip

Part No.

IME 4C Chip Carrier

STC 4P

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Methods

Ø Films or coatings may be applied to the SDE device by dip coating, spin casting, spray painting, air-brushing, brush painting, by Langmuir-Blodgett thin film deposition technique, by electropolymerization, and/or by molecular self assembly.
Ø The chip may be immersed in organic, or aqueous medium to a level above the geometric area occupied by microdiscs.
Ø Electrical contact is made via the bonding pad provided on one end of the long aqxis of the chip. Bonding may be via low temperatre soldering (650-700 C), conductive epoxy,

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Application Notes

For further information, request Application Notes or you may download application note files:
Single Disc Electrodes (SDETM) is the tradename for a family of devices developed by ABTECH. Also called microelectrodes, these devices are microfabricated (using microelectronics fabrication techniques) to form patterns of conductors deposited on an insulating substrate chip.

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Contact: Ann M. Wilson, Manager,
Applications Development ABTECH Scientific, Inc.
800 East Leigh Street, Richmond, Virginia 23219
Telephone Number: +1-804-783-7829 Fax Number: +1-804-783-7830
e-mail: sales@abtechsci.com

Last Revision 04/03/2010, (c) 2000-2010 ABTECH Scientific, Inc.

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